2008年第3期《环境监测管理与技术》目次及主要文章中英文摘要
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2008-06-26
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2008年第3期《环境监测管理与技术》目次
太湖流域生态安全监测体系的构建……………………………………………张宁红(1)
构建南京市现代环境监测体系的思考…………………….唐雅萍,陈宝琳,张丹宁(6)
昆山市环境业务协同管理信息平台的应用及展望……………………………潘文波(9)
主动生物监测技术在水环境风险评价中的应用…………………刘小卫,陆光华(12)
水污染物排放总量控制的体系研究…………………………………杨龙,王晓燕(16)
垃圾填埋场地下水污染对居民健康的风险评价… 段小丽,王宗爽,于云江,等(20)
花垣河锰污染及其成因分析…………………………… 胡南,粟银,秦志峰,等(25)
兰州市西固区域环境空气质量的污染特征………………………………………韦春(28)
琉基葡聚糖凝胶分离富集-二溴对甲偶氮羧微乳液分光光度法测定微量镍 …………………………………………………………陈文宾,王丽萍,马卫兴,等(31)
毛细管低温吸附气相色谱法同时测定空气中痕量甲硫醇和硫化氢 ……………………………………………………………安裕敏,王兴宁,张明时,等(35)
2,4-二硝基苯肼固相吸附/高效液相色谱法测定车内空气中醛酮类物质 ……………………………………………………………赵永刚,胡冠九,宁占武,等(38)
偏振能量色散X射线荧光光谱法测定土壤中金属元素………王平,王焕顺,李玉璞(41)
高效液相色谱法测定土壤中三嗪类除草剂……………………李爱强,陈军,张宗祥(44)
非分散红外线气体法测定生活垃圾填埋气中二氧化碳 …………………………………………………………………宋钊,万方,陈晓婷,等(47)
微波消解-石墨炉原子吸收法测定土壤中钒……………… 陈任翔,刘可,杨力,等(50)
全面建立机动车排气污染监管体系探讨……………王合生, 刘继明, 陈国支(52)
手机获取环境空气监测信息的方法………………………………黄福波,沈学崴(55)
CEMS比对监测要求探讨……………………………………………………… 潘柳青(58)
水样总氮测定空白值偏高的探讨…………………………曹群,孙鸿燕,许士雄(60)
关于加强省级环境监测政务信息工作的思考…………………………………沈颖青(62)
直接显色光度法测定水中硫化物方法改进……………………… 安雅娟,辛天兵(64) 原子吸收光谱法测定酸雨中K、Na、Ca、Mg方法改进……杜青,任兰,陈妍妍(67)
卷件结合整理环境监测档案………………………………………………… 江红(69)
•简讯•(54)(70)
2008年第3期《环境监测管理与技术》主要文章中英文摘要
〖篇 名〗太湖流域生态安全监测体系的构建 〖作 者〗张宁红 〖机 构〗江苏省环境监测中心,江苏 南京 210036 〖摘 要〗针对太湖流域水质污染、湖体富营养化、饮用水质受影响和水生植被减少等生态问题,提出了构建生态安全监测指标体系、布设四类监测点位、引入科学的监测技术与评价体系,从而构建流域生态安全监测体系的设想。 〖关键词〗生态安全;环境监测指标体系; 太湖流域 〖Abstract〗The establishment of ecological safety monitoring indicators system, the four sets of monitoring points, scientific monitoring technology and evaluation system were described for the solution of the water pollution, water body eutrophication, drinking water quality and aquatic vegetation reducing in the Taihu Lake area. 〖Key words〗Ecological safety; Environmental monitoring indicator system; The Taihu Lake area 〖篇 名〗构建南京市现代环境监测体系的思考 〖作 者〗唐雅萍,陈宝琳,张丹宁 〖机 构〗南京市环境监测中心站,江苏 南京 210013 〖摘 要〗简述了在生态文明建设新形势下构建现代环境监测体系的重要性。指出加快能力建设是构建现代环境监测体系的核心,加强网络建设是构建现代环境监测体系的保障,队伍建设是构建现代环境监测体系的根本。提出南京市环境监测要树立大环保观念,通过现代环境监测体系建设,从属地监测向流域监测、区域监测的发展目标。 〖关键词〗生态文明建设; 环境监测体系; 南京市 〖Abstract〗The importance of establishment of the modern environmental monitoring system in the new situation of the ecological civilization was described. The core of the environment monitoring system was accelerated obtaining capability. The monitoring network building ensured the system. The fundament of the system was monitoring staffs. The environmental monitoring should establish the concept of facing whole region. 〖Key words〗 Ecological civilization construction; Environmental monitoring system; Nanjing 〖篇 名〗昆山市环境业务协同管理信息平台的应用及展望 〖作 者〗潘文波 〖机 构〗昆山市环境科学保护研究所,江苏 昆山 215300 〖摘 要〗简述了环境业务协同管理信息平台开发目的、系统结构、系统管理、系统组成,以及系统在污染源普查中的应用。提出扩展系统功能,实现对节能减排、污染源普查等与环境管理深层次要求相适应的环境管理信息系统建设的展望。 〖关键词〗环境管理; 信息系统; 污染源普查; 昆山市 〖Abstract〗The purpose, structure, management and composition of the environmental management information system platform was described. The establishment of environmental management information system should be suitable for applications of energy saving, census of pollution source and Environmental management. 〖Key words〗Environmental management; Information system; Census of pollution source; Kunshan 〖篇 名〗主动生物监测技术在水环境风险评价中的应用 〖作 者〗刘小卫1,陆光华2 〖机 构〗1.河海大学公共管理学院,江苏 南京 210098; 2.浅水湖泊综合治理与资源开发教育部重点实验室,河海大学环境科学与工程学院,江苏 南京 210098 〖摘 要〗采用生物监测技术综合分析污染物的环境行为和污染诱导的生物学效应,用于评估和预测水环境中化学品的生态风险,对保护有限的水资源和维持生态系统健康具有重要意义。介绍了主动生物监测的概念、操作流程,以及相对传统的被动生物监测所具有的优势,综述了主动生物监测技术在海洋和淡水环境质量监测中常用的指示生物,以及能对不同污染物作出响应的各种生物标志物,讨论了该领域国内外的最新研究进展。 〖关键词〗主动生物监测;指示生物;生物标志物;生态风险 〖Abstract〗 The environmental action of pollutants and pollutioninduced biological effects were comprehensively analyzed with biological monitoring techniques for ecological risks assessment and forecast of water environmental chemicals. It is important for protection of the limited water resources and maintenance of ecosystem health. The concept of active biological monitoring, operational procedures and the advantages of relatively traditional passive biological monitoring were introduced. The commonly used bioindicators in environmental quality of marine and freshwater in active biomonitoring technology were summarized as well as biomarkers responding to different pollutants. The latest developments of research in the field at home and abroad were discussed. 〖Key words〗Active biomonitoring; Bioindicator; Biomarker; Ecological risk 〖篇 名〗水污染物排放总量控制的体系研究 〖作 者〗杨龙, 王晓燕 〖机 构〗首都师范大学资源环境与旅游学院,北京 100037 〖摘 要〗回顾了我国水污染物排放总量控制发展的历程,针对总量控制方法体系中存在的问题,将非点源污染和不确定性分析纳入总量控制研究,构建了新的水污染总量控制方法系统,并对方法体系涉及的管理基础、管理目标、管理模型和管理实施等问题进行了研究。 〖关键词〗总量控制;非点源污染;不确定性信息;水质模型;最大日负荷总量 〖Abstract〗On the Chinese development of total amount of pollutants control in waste water,the new system was established to lay heavy stress on existing problems for the control. The nonpoint source pollution and uncertainty analysis were brought into the system research. The problems involved in the management itself, objectives, model and implementation and other issues of the system were discussed. 〖Key words〗Total amount of pollutants control; Nonpoint source pollution; Unascertained information; Water quality model; Total maximum daily loads 〖篇 名〗垃圾填埋场地下水污染对居民健康的风险评价 〖作 者〗段小丽,王宗爽,于云江,聂静,王菲菲,赵秀阁 〖机 构〗 中国环境科学研究院,北京 100012 〖摘 要〗调查了某垃圾填埋场地下水和周边居民饮用水中的As、Hg等重金属和挥发酚等有机物的污染状况,运用美国环保局的健康风险计算模型,评估了该垃圾填埋场地下水对周边居民的潜在健康风险。结果表明,各类人群对4种有阈化合物的饮食和皮肤暴露的终身健康危险度在8.2×10-11~1.3×10-10之间,均低于可以接受的风险水平10-6;对As的终身超额健康危险度在3.1×10-7~4.9×10-7之间,表明地下水中砷污染对居民潜在的致癌风险不明显。各类人群通过皮肤对Hg、As、Cd和挥发酚的暴露剂量比通过饮水暴露的剂量高0.7倍~14.5倍,皮肤暴露将是地下水影响人体健康并构成潜在风险的重要途径。 〖关键词〗垃圾填埋场;地下水;污染物;健康风险; 暴露剂量; 危险度评估 〖Abstract〗The pollution of heavy metals such as arsenic, mercury and volatile phenols were investigated on the underground water near a landfill site and drinking water. The potential risk assessments of the underground water and drinking water were estimated by US EPA health risk assessment model. The results showed that the lifetime health risks of research subjects through dietary intake and dermal exposure to 4 nonthreshold compounds were 8.2×10-11~1.3×10-10, lower than the acceptable risk level 10-6. Their excess lifetime risk to arsenic was 3.1×-7~4.9×-7. It was revealed from this study that the dermal exposure seems to a dominant exposure route for human health risk. The exposure doses of research subjects through cutaneous contact to mercury, arsenic, chromium and volatile phenols were 0.7~14.5 times to the doses through dietary intake. 〖Key words〗Landfill site; Underground water; Pollutant; Health risk assessment; Exposure dose; Risk assess
〖篇 名〗花垣河锰污染及其成因分析 〖作 者〗胡南1, 粟银2, 秦志峰1,吴彦琼1, 郑济芳1 〖机 构〗1.南华大学生命科学与技术学院,湖南 衡阳 421001;2.吉首大学生物资源与环境科学学院,湖南 吉首 416000 〖摘 要〗对花垣河河水中8个监测断面(S1—S8)水样和堆积在河岸附近MnSO4废渣及其浸出液中Mn、Cd、Pb、Cu和Zn等5种重金属元素的总量进行了分析。结果表明,花垣河河水中Mn和Cd质量浓度超过《地表水环境质量标准》(GB 3838-2002)Ⅴ类水体标准;MnSO4废渣浸出液中Cd超过《危险废物鉴别标准》(GB 5058.3-1996)规定值。将花垣河河水中Mn、Cd、Pb、Cu和Zn的含量与MnSO4废渣浸出液中相应的元素含量进行相关性分析,r=0.957(p<0.01),表明堆积在花垣河河岸附近MnSO4废渣是可能造成花垣河污染的主要来源。 〖关键词〗重金属污染;MnSO4废渣;废渣堆场;花垣河 〖Abstract〗The concentrations of metals Such as Mn, Cd, Pb, Cu, and Zn in the water sample collected from 8 sites (S1—S8) and the solutionions in the manganese sulphate waste residue deposited along the Huayuan River were determined. The results showed that the levels of Mn and Cd were over the China environmental quality standards for surface water(GB 3838-2002). The levels of Mn, Cd, Cu and Zn in the leaching out liquid of manganese sulphate waste residue were over the China integrated wastewater discharge standard guideline(GB 5058.3-1996). A significant positive correlation of the average concentration of Mn, Cd, Pb, Cu, and Zn was obtained between the Huayuan River and the leaching out liquid of manganese sulphate waste residue (r=0.957, p<0.01) by corresponding analysis . The Huayuan River pollution may be caused by the MnSO4 residue. 〖Key words〗Metals polluution; Manganese sulphate waste residue; Wwaste residue dumping; Huayuan River
〖篇 名〗琉基葡聚糖凝胶分离富集-二溴对甲偶氮羧微乳液分光光度法测定微量镍 〖作 者〗陈文宾1,2,王丽萍1,2,马卫兴2,许兴友2,徐国想2 〖机 构〗1.中国矿业大学环境与测绘学院,江苏 徐 州 221008; 2.淮海工学院化学工程系,江苏 连云港 222005) 〖摘 要〗研究了在溴代十六烷基吡啶(CPB)、正丁醇、正庚烷、水自制微乳溶液存在下,镍与二溴对甲偶氮羧(DBpMCA)的显色反应,在pH值为9.07的Na2B4O7-HCl缓冲溶液中,镍与试剂形成淡红色配合物,最大吸收峰位于560 nm波长处,表观摩尔吸光系数ε为2.8×105 L/(mol•cm)。优化了试验条件,考察了共存离子的影响,方法在0.002 mg/L~0.320 mg/L范围内符合比尔定律,检出限为0.000 6 mg/L,生活垃圾、水、土壤样品测定的RSD为2.1%~5.2%,加标回收率为96.6%~104%。 〖关键词〗镍;琉基葡聚糖凝胶;二溴对甲偶氮羧;分光光度法 〖Abstract〗The color reaction of the reagent Dibromopmethyl carboxyazo(DBpMCA) with nickel in the presence of micromulsion Cetyl Pyridine Bromide(CPB)、nC4H9OH、C7H14、H2O were studied. Results showed that the color reagent with nickel and DBpMCA microemulsiom formed a stable light red complex in the medium of Na2B4O7HCl buffer at pH 9.07. The maximum absorption wavelength and apparent molar absorptivity were 560 nm and 2.8×105 L/(mol•cm) respectively. The test parameters were optimized and influence of coexist ions was observed. Beer′s Law was obeyed in the range of 0.002 mg/L~0.320 mg/L for nickel. The detection limit was 0.000 6 mg/L. The RSD and recovery were 2.1%~5.2% and 96.6%~104% in water ,domestic waste and soil samples. 〖Key words〗 Nickel; Mercaptodextrangel; Dibromopmethyl carboxyazo(DBpMCA); Spectrophometry
〖篇 名〗毛细管低温吸附气相色谱法同时测定空气中痕量甲硫醇和硫化氢 〖作 者〗安裕敏1,王兴宁2,张明时2,曹桂红2 〖机 构〗1.贵州省环境科学研究设计院,贵州 贵阳 550002;2.贵州师范大学,贵州省山地环境重点实验室,贵州 贵阳 550001 〖摘 要〗建立了毛细管低温吸附气相色谱同时测定空气中痕量甲硫醇和硫化氢的方法,介绍了冷冻吸附装置的制备方法和样品冷凝吸附流程。甲硫醇和硫化氢分别在0.467 ng~5.16 ng和0.327 ng~3.60 ng范围内线性良好,当进样体积为1 L时,检出限为0.205 μg/m3和0.213 μg/m3,空白加标平均回收率为88.6%和90.2%,RSD为6.0%和6.5%。 〖关键词〗甲硫醇;硫化氢;毛细管;低温吸附;气相色谱法;空气 〖Abstract〗 The method of a lowtemperature adsorption capillary GC was established for determination of trace methyl mercaptan and hydrogen sulfide in the air. The sample preparation method of frozen adsorption devices and condensate absorption process were described. The good linearities were achieved in methyl mercaptan at 0.467 ng~5.16 ng and in hydrogen sulfide at 0.327 ng~3.60 ng. The detection limit of methyl mercaptan was 0.205 μg/m3, and detection limit of hydrogen sulfide was 0.213 μg/m3 for 1 L sample. The average blank recoveries were 88.6% and 90.2%, RSD were 6.0% and 6.5% respectively. 〖Key words〗Methyl mercaptan; Hydrogen sulfide; Capillary; Cryogenic adsorption; Gas chromatography; Air
〖篇 名〗2,4-二硝基苯肼固相吸附/高效液相色谱法测定车内空气中醛酮类物质 〖作 者〗赵永刚1,胡冠九1,2,宁占武3,张祥志1,章勇1,周春宏1 〖机 构〗1.江苏省环境监测中心,江苏 南京 210036; 2.南京大学环境学院,污染控制与资源化研究国家重点实验室,江苏 南京 210093; 3.北京市劳动保护科学研究所,北京 100054 〖摘 要〗建立了2,4-二硝基苯肼固相吸附/高效液相色谱同时测定车内空气中4种醛酮类物质的方法,研究了固相吸附采样和前处理方法,优化了试验条件。4种醛酮类物质在一定质量范围内工作曲线线性良好,甲醛、乙醛、丙烯醛、丙酮的检出限分别为0.075 μg/m3、0.207 μg/m3、0.715 μg/m3、0.159 μg/m3(按采样体积12 L计),实际样品测定的RSD为7.5%~9.7%。 〖关键词〗醛酮类物质;2,4-二硝基苯肼;固相吸附;高效液相色谱法;车内空气 〖Abstract〗A method was established for determining the four Formaldehydes including formaldehyde, acetaldehyde, acrolein and acetone. The adsorbents and pretreatment were tested and parameters were optimized. The good linearities of the four compounds were achieved. The limits of detection of formaldehyde, acetaldehyde, acrolein and acetone were 0.075 μg/m3, 0.207 μg/m3, 0.715 μg/m3 and 0.159 μg/m3 by 12 liters sampling air. The RSD were from 7.5% to 9.7%. 〖Key words〗 Aldehydes and Ketones; 2,4-DNPH; Soild phase extraction; HPLC; Air inside car 〖篇 名〗偏振能量色散X射线荧光光谱法测定土壤中金属元素 〖作 者〗王平,王焕顺,李玉璞 〖机 构〗大连市环境监测中心,辽宁 大连 116023 〖摘 要〗建立了偏振能量色散X射线荧光光谱同时测定土壤中6种金属元素的方法,优化了试验条件。方法线性良好,Cr、Mn、Pb、Cu、As、Se的检出限分别为3.62 mg/kg、3.65 mg/kg、0.91 mg/kg、0.23 mg/kg、0.35 mg/kg、0.01 mg/kg,土壤标准样品的测定结果均符合要求,实际样品测定的RSD为0.5%~10.0%,与原子吸收法、原子荧光法的测定结果相吻合。 〖关键词〗偏振能量色散;X射线荧光光谱法;金属元素;土壤 〖Abstract〗A method was established by polarized radiationenergy dispersive Xray fluorescence spectrometry to determine six metal elements simultaneously. The test parameters were optimized and good linearities were achieved. The detection limits of Cr, Mn, Pb, Cu, As, Se were 3.62 mg/kg, 3.65 mg/kg, 0.91 mg/kg, 0.23 mg/kg, 0.35 mg/kg and 0.01 mg/kg separately. The test results of the soil standard samples met the requirement. The RSD of practical samples were from 0.5% to 10.0%, and equaled to results of AAS, AFS tests.〖JP〗 〖Key words〗Polarized radiation energy dispersion; Xray fluorescence spectrometry; Metal elements; Soil 〖篇 名〗高效液相色谱法测定土壤中三嗪类除草剂 〖作 者〗李爱强,陈军,张宗祥 〖机 构〗泰州市环境监测中心站,江苏 泰州 225300 〖摘 要〗建立了索氏提取、中性氧化铝小柱净化、高效液相色谱二极管阵列检测器测定土壤中7种三嗪类除草剂的方法,优化了检测波长、提取方法和溶剂、梯度淋洗程序等试验条件。7种三嗪类除草剂在0.10 mg/L~2.00 mg/L范围内线性良好,检出限为0.84 μg/kg~2.07 μg/kg,RSD为1.2%~5.6%,加标回收率为95.0%~107%。 〖关键词〗三嗪类除草剂;高效液相色谱法;索氏提取;土壤 〖Abstract〗A HPLC with PDAD, soxlet extraction and neutral alumina clean up cartridge method was established for the simultaneous determination of seven triazine herbicides in the soil. The detection wavelength, solvent and extraction methods, procedures of gradient leaching were optimized. The good linearities of the 7 triazine herbicides were achieved in 0.10 mg/L~2.00 mg/L. The detection limits were 0.84 μg/kg ~2.07 μg/kg, RSD 1.2%~5.6%, and the recoveries 95.0%~107%. 〖Key words〗Triazine herbicides; HPLC; Soxlet extraction; Soil 〖篇 名〗非分散红外线气体法测定生活垃圾填埋气中二氧化碳 〖作 者〗宋钊,万方,陈晓婷,陈斌 〖机 构〗上海市环境监测中心,上海 200030 〖摘 要〗采用非分散红外线气体法测定生活垃圾填埋气中的二氧化碳,介绍了填埋气监测井的设置及样品采集和测定方法,讨论了稀释倍数、配气方法和填埋气成分对测定的影响,经验证,方法准确度和精密度均符合要求。 〖关键词〗二氧化碳;非分散红外线气体法;生活垃圾;填埋气 〖Abstract〗The Non dispersive Infrared method was used to determine the carbon dioxide in landfill gas. The landfill gas monitoring wells, sample collection and testing methods were described. The influences of diluted multiples, standard gases mixed method and composition of landfill gases were discussed. 〖Key words〗Carbon dioxide; Nondispersive Infrared method; Garbage; Landfill gas 〖篇 名〗微波消解-石墨炉原子吸收法测定土壤中钒 〖作 者〗陈任翔,刘可,杨力,陈瑶 〖机 构〗湘潭市环境保护监测站,湖南 湘潭 411104 〖摘 要〗建立了微波消解-石墨炉原子吸收测定土壤中钒的方法,优化了微波消解程序。方法在0 μg/L~100 μg/L范围内线性良好,以称样0.500 0 g、定容体积50 mL计,方法检出限为0.2 μg/g,环境土壤标准样品测定的RSD为2.5%,加标回收率为92.0%~104%。 〖关键词〗钒;微波消解;石墨炉原子吸收法;土壤 〖Abstract〗The determination method of vanadium in soil was established by microwave digestion-GFAAS. The microwave digestion process was optimized. The linearity from 0 μg/L to 100 μg/L was good. The detection limit was 0.2 μg/g by 0.500 0 g soil sample and the volume capacity of 50 mL, the RSD 2.5% and the recoveries from 92.0% to 104% in the environmental standards soil samples test. 〖Key words〗Vanadium; Microwave digestion; GFAAS; Soil 〖篇 名〗全面建立机动车排气污染监管体系探讨 〖作 者〗王合生, 刘继明, 陈国支 〖机 构〗南京市环境监测中心站,江苏 南京210013 〖摘 要〗对南京市机动车排气污染监督管理工作进行了分析,指出了存在的问题,设计了未来监督管理工作的思路。提出对机动车排气污染监管要构建完整的监管体系,重在对部门的监管;加强车辆使用全过程污染防治监管,建立对各级机动车维修企业尾气治理行为的监管制度;启用严格的排放标准和检测手段,全面控制机动车排气污染。 〖关键词〗机动车; 污染排放; 监督管理 〖Abstract〗The situation and problems of vehicle exhaust pollution supervision and management in Nanjing was briefly described. The ideas of the future work was proposed.The establishment of a complete supervision and control system for vehicle exhaust pollution should put its main force on divisional management. The entire process of pollution control and prevention in use of vehicles should be strengthen. Exhaust gas control regulation to all vehicle maintenance corporations should be established. Strict exhaust Standards and testing methods should be used for control of vehicle exhaust pollution. 〖Key words〗Vehicle; Pollution exhaust; Supervision and management 〖篇 名〗手机获取环境空气监测信息的方法 〖作 者〗黄福波,沈学崴 〖机 构〗大连市环境监测中心,辽宁 大连 116023 〖摘 要〗为满足了社会公众实时查询区域空气污染物实时状况和日变化,监测点空气污染指数和对应的SO2、NO2、CO、PM10的质量浓度,以及气象信息、空气质量日报、预报信息的需求,基于KJAVA在嵌入式系统上的应用技术,建立了手机GPRS无线通信环境空气质量信息查询分析系统。 〖关键词〗空气污染信息;环境监测; 无线分组业务;手机 〖Abstract〗Based on the application technology of KJAVA on the inserted type system, information inquiry analysis system of the ambient air quality was established by GPRS wireless communication of mobile phone. The system meets the citizen to know the daily variation of air pollutants in the air and air pollution index of environmental monitoring substations and corresponding mass concentrations of SO2, NO2, CO, PM10 as well as meteorological information, air quality daily report, forecast information. 〖Key words〗 Air pollution information; Environmental monitoring; GPRS ;Mobile phone 〖篇 名〗CEMS比对监测要求探讨 〖作 者〗潘柳青 〖机 构〗柳州市环境监测站,广西 柳州 545001 〖摘 要〗根据《固定污染源烟气排放连续监测系统技术规范(试行)》(HJ/T 75-2007)分析实际监测中遇到的问题,提出了该技术规范在适用性方面需要明确的事项。指出应事先规范比对监测中可能遇到的数据处理及结果判断问题,从规避法律风险的角度出发,对比对监测进行文件控制和档案管理。 〖关键词〗固定污染源;烟气排放连续监测系统;比对监测 〖Abstract〗The “HJ / T 75-2007 Technical Specification for Fixed Polluting Gasous Sources Continuous Emission Monitoring System (draft)” was discussed for practical environmental monitoring. The key in the technical specifications was required for clear and the data processing and the results of judgment in the comparative monitoring should be standardization to avoid legal risks of the comparative monitoring by the document control and records management. 〖Key words〗Stationary pollution sources; Continuous emission monitoring system; Comparative monitoring 〖篇 名〗水样总氮测定空白值偏高的探讨 〖作 者〗曹群, 孙鸿燕, 许士雄 〖机 构〗南昌航空大学环境与化学工程学院,江西 南昌 330063 〖摘 要〗根据《水质总氮的测定碱性过硫酸钾消解紫外分光光度法》(GB 11894-89)测定地表水中的总氮时,空白试验的吸光值常偏高。经对加热消解时间、试验用水水质、试剂添加顺序、储存时间等因素进行了试验,并对操作步骤影响吸光度空白值作了探讨。 〖关键词〗总氮; 空白实验; 吸光度; 过硫酸钾氧化-紫外分光光度法 〖Abstract〗The higher absorbance of blank test was observed at the determination of total nitrogen in surface water by Water QualityTotalnitrogen DeterminationK2S2O8 Oxidization Ultraviolet Spectrometry (China National Standard 11894-89). The influencing factors were tested such as time of heat digestion, quality of lab water, addition order and storage of reagents. The test steps to influence absorbance blank value was also discussed. 〖Key words〗Total nitrogen;Blank test; Absorbance;K2S2O8 oxidizationultraviolet spectrometry 〖篇 名〗原子吸收光谱法测定酸雨中K、Na、Ca、Mg方法改进 〖作 者〗杜青, 任兰, 陈妍妍 〖机 构〗南京市环境监测中心站,江苏 南京 210013 〖摘 要〗用0.1%硝酸溶液配制混合标准溶液,不加抗干扰试剂,火焰原子吸收光谱法直接测定酸雨中K、Na、Ca、Mg,方法精密度、准确度满足酸雨监测的分析要求。 〖关键词〗钾; 钠; 钙; 镁; 酸雨; 原子吸收光谱法 〖Abstract〗The standard solution was prepared by 0.1 percent nitric acid, no any anti interference reagents needed. The potassium, sodium, calcium and magnesium in acid rain were determined by FAAS. The accuracy and precision of the improved method meted the requirements of acid rain monitoring. 〖Key words〗 Potassium; Sodium; Calcium; Magnesium; Acid rain; Atomic absorption spectrometry 〖篇 名〗卷件结合整理环境监测档案 〖作 者〗江红 〖机 构〗温州市环境监测中心站,浙江 温州325003 〖摘 要〗分析了环境监测档案管理特点,提出改卷为件和卷件结合开展档案归档整理的思路与方法。划分出直接改卷为件整理和采用组件与虚拟卷整理的环境监测档案类别。提出了将卷件结合整理与改卷为件的档案纳入同一个编号体系管理的办法。 〖关键词〗环境监测;档案管理;案卷 〖Abstract〗According to File Management Regulation and environmental monitoring files characteristic, the file management pattern should change from the volume to the paper combined volume. The environmental monitoring file categories should chassify into direct paper management and virtual volume management. The file managements of the volume and the paper combined volume use an identical serial number system. 〖Key words〗Environmental monitoring; File management; File volume
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